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Product |
Yield,% |
B.P., °C./mm. |
nD (t, °C) |
---|---|---|---|
44 |
104–105/40 |
1.5701 (22) |
|
66 |
92–93/16 |
— |
|
58 |
149–151/40 |
1.5212 (25) |
|
67 |
120–121/40 |
1.5557 (25) |
|
69 |
125–127/40 |
1.5451 (23) |
|
77 |
141–142/40 |
1.5799 (25) |
|
Appendix
Compounds Referenced (Chemical Abstracts Registry Number)
amine
Trimethyl and triethyl orthoformate
aceto-p-chloroanilide
ethanol (64-17-5)
calcium chloride (10043-52-4)
potassium carbonate (584-08-7)
sulfuric acid (7664-93-9)
hydrochloric acid (7647-01-0)
ether (60-29-7)
Ethyl bromide (74-96-4)
potassium hydroxide (1310-58-3)
triethyl orthoformate (122-51-0)
N-Methylaniline (100-61-8)
lithium aluminum hydride (16853-85-3)
N-Ethylaniline (103-69-5)
p-chloroaniline (106-47-8)
N-Ethyl-m-toluidine (102-27-2)
N-Ethyl-p-chloroaniline, Aniline, p-chloro-N-ethyl- (13519-75-0)
N-Ethyl-p-chloroformanilide (26772-93-0)
ethyl N-p-chlorophenylformimidate
N-Methyl-m-toluidine (696-44-6)
N-Methyl-p-chloroaniline (932-96-7)